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Total Synthesis and Stereochemistry Assignment of Nucleoside Antibiotic A-94964.
Shao, Xiaofei; Zheng, Chang; Xu, Peng; Shiraishi, Taro; Kuzuyama, Tomohisa; Molinaro, Antonio; Silipo, Alba; Yu, Biao.
Afiliação
  • Shao X; School of Chemistry and Materials Science, Hangzhou Institute for Advanced Study, University of Chinese Academy of Sciences, Hangzhou, China.
  • Zheng C; State Key Laboratory of Bioorganic and Natural Products Chemistry, Center for Excellence in Molecular Synthesis, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, Shanghai, China.
  • Xu P; School of Chemistry and Materials Science, Hangzhou Institute for Advanced Study, University of Chinese Academy of Sciences, Hangzhou, China.
  • Shiraishi T; State Key Laboratory of Bioorganic and Natural Products Chemistry, Center for Excellence in Molecular Synthesis, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, Shanghai, China.
  • Kuzuyama T; Graduate School of Agricultural and Life Sciences, The University of Tokyo, Tokyo, Japan.
  • Molinaro A; Graduate School of Agricultural and Life Sciences, The University of Tokyo, Tokyo, Japan.
  • Silipo A; Collaborative Research Institute for Innovative Microbiology, The University of Tokyo, Tokyo, Japan.
  • Yu B; Department of Chemical Sciences, University of Naples Federico II, Napoli, Italy.
Angew Chem Int Ed Engl ; 61(14): e202200818, 2022 03 28.
Article em En | MEDLINE | ID: mdl-35142022
A collective total synthesis of eight diastereoisomers associated with NMR analysis leads to a full stereochemistry assignment of the structurally unique nucleoside antibiotic A-94964, which features an octuronic acid uridine core decorated with an α-D-mannopyranosyl residue and an α-D-N-acylglucosaminopyranosyl residue via a phosphodiester bridge.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Antibacterianos / Nucleosídeos Idioma: En Revista: Angew Chem Int Ed Engl Ano de publicação: 2022 Tipo de documento: Article País de afiliação: China País de publicação: Alemanha
Texto completo
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XML
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Antibacterianos / Nucleosídeos Idioma: En Revista: Angew Chem Int Ed Engl Ano de publicação: 2022 Tipo de documento: Article País de afiliação: China País de publicação: Alemanha