Detection of multiple endocrine-disrupting chemicals in milk: Improved and safe high performance liquid chromatography tandem mass spectrometry method.
J Sep Sci
; 45(9): 1538-1549, 2022 May.
Article
em En
| MEDLINE
| ID: mdl-35182112
ABSTRACT
Herein, an improved method for detecting the endocrine-disrupting chemicals in milk is presented, which is based on high performance liquid chromatography tandem mass spectrometry, coupled with a quick, effective, and safe method. The linearity of the proposed method was in the range of 0.05-100 µg/L, and all correlation coefficients were ≥0.9973. At three concentration levels, the spiked recoveries ranged from 77.7 to 107.5%, relative standard deviations ranged from 0.2 to 14.6%, limits of quantitation ranged from 0.1 to 40 µg/kg, limits of detection ranged from 0.03 to 13.3 µg/kg. The proposed method for the identification and quantitation of 26 endocrine disruptors present in milk is not only easy, fast, and cost-efficient but also provides a reference for the detection of various endocrine disruptors in milk and other dairy products.
Palavras-chave
Texto completo:
1
Coleções:
01-internacional
Base de dados:
MEDLINE
Assunto principal:
Disruptores Endócrinos
Tipo de estudo:
Diagnostic_studies
Limite:
Animals
Idioma:
En
Revista:
J Sep Sci
Ano de publicação:
2022
Tipo de documento:
Article