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A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid.
Wang, Yi; Sun, Mengting; Gao, Zhanyang; Zou, Lilin; Zhong, Lingyu; Peng, Ruichao; Yu, Ping; Luo, Yunbai.
Afiliação
  • Wang Y; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Sun M; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Gao Z; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Zou L; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Zhong L; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Peng R; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Yu P; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
  • Luo Y; Engineering Research Center of Organosilicon Compounds & Materials, Ministry of Education, College of Chemistry and Molecular Sciences, Wuhan University Wuhan 430072 P. R. China ybai@whu.edu.cn.
RSC Adv ; 8(65): 37159-37164, 2018 Nov 01.
Article em En | MEDLINE | ID: mdl-35557811
A novel synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid which has mild conditions and low toxicity is described. This study introduces detailed synthetic protocols and characterization including GC-MS, 13C NMR and 19F NMR spectroscopy of perfluoroisobutyryl acid, perfluoroisobutyryl chloride, perfluoroisobutyl amide and perfluoroisobutyronitrile. Besides, this route is superior to the established patent and shows potential application in high voltage electrical equipment.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: RSC Adv Ano de publicação: 2018 Tipo de documento: Article País de publicação: Reino Unido
Texto completo
Adicionar na Minha BVS
Imprimir
XML
PubMed Links
Buscar no Google

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Revista: RSC Adv Ano de publicação: 2018 Tipo de documento: Article País de publicação: Reino Unido